Contents of 17 Metal Elements in Food Determined by Inductively Coupled Plasma Atomic Emission Spectrometry

Determination of thirteen common elements in food samples by inductively coupled plasma atomic emission spectrometry: comparison of five digestion methods.

Five sample digestion procedures were evaluated for the determination of Al, B, Ca, Cu, Fe, K, Mg, Mn, Na, P, S, Sr, and Zn in food samples by inductively coupled plasma atomic emission spectrometry. The 5 procedures include dry ashing at 500 degrees C, wet digestion with HNO3-HClO4, microwave digestion with HNO3, microwave digestion with HNO3-H2O2, and microwave digestion with HNO3-H2O2-HF. Fo...

Selective Separation and Preconcentration of trace Amounts of Gallium in Water and Rice Samples using Cloud Point Extraction and Determination by Inductively Coupled Plasma-Atomic Emission Spectrometry

In the present study a cloud-point extraction process using non-ionic surfactant Triton X-114 for selective extraction of gallium from aqueous solutions was developed. The method is based on the complex formation of Ga (III) with N, N′ -bis (salycilidene)-1, 2-phenylenediamine (salophen) as a chelating agent in buffer media of pH 5. After phase separation and dilution of the surfactant-rich pha...

Inductively Coupled Plasma - Optical Emission Spectrometry

ACKNOWLEDGEMENTS INTRODUCTION CONTENTS 1.1 Forensic Science Investigations 1.2 Forensic Science Analysis 2 1.3 Inductively Coupled Plasma-Optical Emission Spectrometry 7 1.4 The Aims of This Investigation 8 2 INDUCTIVELY COUPLED PLASMA-OPTICAL EMISSION SPECTROMETRY 10 2 .l Introduction 2.2 The Inductively Coupled Plasma 2.3 Instrumentation Used in This Study 2.3.1 Radio Frequency Generator 2.3....

Inductively Coupled Plasma/Optical Emission Spectrometry

Determination of titanium and vanadium in Ziegler-Natta catalysts by inductively coupled plasma atomic emission spectrometry.

A method for the determination of Ti and V using inductively coupled plasma atomic emission spectrometry (ICP OES) in Ziegler-Natta polymerization catalysts is proposed. The concentrations of both Ti and V are efficiently determined after catalyst acid digestion with a mixture of HNO3 + HCl + HF and heating (160 degrees C for 6 h) or with 10% (v/v) H2SO4 and heating (160 degrees C for 6 h) or w...